Re: ORGLIST: Everybody Digest, Vol 48, Issue 2

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From: Srinath T. (meetnandhu$##$yahoo.com)
Date: Wed Jun 04 2008 - 16:42:17 EDT


Hi Rosanna,

How about using Na/liq.NH3? There is plenty of literature available on that.

Srinath

--- On Wed, 6/4/08, everybody-request$##$orglist.net <everybody-request$##$orglist.net> wrote:
From: everybody-request$##$orglist.net <everybody-request$##$orglist.net>
Subject: Everybody Digest, Vol 48, Issue 2
To: everybody$##$orglist.net
Date: Wednesday, June 4, 2008, 1:00 PM

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Today's Topics:

   1. Re: Dibenzylamine (ling huang)
   2. 2-Amino-4-methoxy-benzoic acid methyl ester (Kishore Babu Ch)

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Message: 1
Date: Mon, 2 Jun 2008 15:18:48 -0700 (PDT)
From: ling huang <ling.huang$##$prodigy.net>
Subject: Re: ORGLIST: Dibenzylamine
To: Rossana Ferrara <rossana.ferrara$##$unimi.it>, everybody$##$orglist.net
Message-ID: <464452.42728.qm$##$web83803.mail.sp1.yahoo.com>
Content-Type: text/plain; charset="iso-8859-1"

Hi Rossana,
                      It is done with hydrogenation in MeOH. Have you tried
with different catalysts?
   
  Ling Huang
  Chemistry Department
  Sacramento City College
  http://www.freewebs.com/huangl24
  http://www.scc.losrios.edu

Rossana Ferrara <rossana.ferrara$##$unimi.it> wrote: Dear all,
i need to debenzylate dibenzylamine. I know that i can do it with hydrogenation
in MeOH but my reaction doesn't work(maybe the problem is that i have
in my product other free amine that probably don't allow the normal way of
reaction). I tried to do the reaction in acetic acid but i had some trouble
anyway. Do you have any advise?
Thanks a lot
Rossana

  Rossana Ferrara
PhD student
Universit? degli studi di Milano

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Message: 2
Date: Wed, 4 Jun 2008 04:11:08 -0700 (PDT)
From: Kishore Babu Ch <kbchilukuri$##$yahoo.com>
Subject: ORGLIST: 2-Amino-4-methoxy-benzoic acid methyl ester
To: everybody$##$orglist.net
Message-ID: <670976.24218.qm$##$web50604.mail.re2.yahoo.com>
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hi friends,
 
how to prepare 2-Amino-4-methoxy-benzoic acid methyl ester, if any reference
please give me mail
 
thanks
 
ch.k

      
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