ORGLIST: Safety -Synthesis of EDC-HCl

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From: paul joshua (pauljoshua_in$##$yahoo.com)
Date: Mon Feb 27 2006 - 03:02:50 EST


Dear all,
  Could anybody help me the safety precautions that need to be taken while Synthesising
  n-(3-Dimethylaminopropyl)-N-ethylcarbodimmide Hydrochloride or EDC-HCl.
  Starting from Ethyl isocyanate and N,N -Dimethyl-1,3-Propanediamine.
  Ref: Org Syn ,Coll.Vol.5,p.555(1973); vol.48,p.83 (1968)
  CAS 25952-53-8
  Thanx in advance
  Regards-
  Paul

                      
S.Paul Joshua

    
  
  The great tragedy of science -- the slaying of a beautiful hypothesis by an ugly fact.
--Thomas Huxley

                
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