ORGLIST: thiol with Nitrobenzyl chloride

From: srinivas reddy (gounisrinivas$##$yahoo.com)
Date: Fri Feb 17 2006 - 10:33:30 EST

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Dear all,

I tried to make thiol from p-nitrobenzyl chloride and
thiourea. in the past i prepared few thiols with
benzyl chlorides derivatives, all of them were
liquids. but in this case it seems the reaction did
not worked well to give a thiol. i feel that
p-nitrobenzyl chloride (is a solid) might have formed
some other compound rather than thiouronium salt hence
it was difficult in breaking with NaoH to form thiol.
any suggestions please?.

thanks in advance

regards

Srinivas

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