Re: ORGLIST: Reductive Amination

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From: Sengen Sun (sengensun$##$yahoo.com)
Date: Fri Feb 03 2006 - 16:39:19 EST

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In reply to: shrent: "ORGLIST: Reductive Amination"

A ketone can be converted to a primary amine by NH4Ac
and NaBH3CN in MeOH. You may heat the reaction to 60
oC in a pressure bottle to make it faster.

Journal of Medicinal Chemistry, 1994, 37, 913-923.

Other method: Tetrahedron Letters 1990, 31, 5547-5550.

Sengen

--- shrent <shrent$##$rediffmail.com> wrote:

>
> Hi !
>
> Can I get advices regarding Direct conversion of a
> methyl-cyclo-aliphatic Ketone to its Primary Amine
> with commercial reagents ? It is based on Reductive
> Amination.
>
> Awaiting your suggetions !
>
>
>
> Regards,
> shrent >
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In reply to: shrent: "ORGLIST: Reductive Amination"

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