RE: ORGLIST: how to increase yield of Thiol

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From: JohnSRoberts (JohnSRoberts$##$worldnet.att.net)
Date: Fri Jan 27 2006 - 09:47:39 EST


No, but the easiest method for making the various benzyl mercaptans from
benzyl chlorides is to run the reaction in aqueous NaSH with excess hydrogen
sulfide (under hydrogen sulfide pressure).

-----Original Message-----
From: everybody-bounces$##$orglist.net [mailto:everybody-bounces$##$orglist.net]
On Behalf Of srinivas reddy
Sent: Thursday, January 26, 2006 7:06 PM
To: everybody$##$orglist.net
Subject: ORGLIST: how to increase yield of Thiol

 Hi,

does anyone know the procedure/literature reference to
increase the yields of thiols which are obtained by
reacting benzyl chloride derivatives and thiourea.

thanks in advace

Srinivas
        

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