From: Deepak Shukla (DEEPAK.SHUKLA2$##$ranbaxy.com)
Date: Wed Aug 17 2005 - 01:23:24 EDT
Hi everybody,
While working on safe methods for THF and Ethyl acetate moisture removal , A lot of good literature is available in Solvent recovery and safety handbooks e.g.. by Smallwood and on different web sites but I am searching some good literature on two subjects,
1.In case of THF either pervaporation or Caustic followed by molecular sieves treatment the peroxide content is becoming an unavoidable danger. We have been using peroxide inhibitors in all stages still if somebody could share some reference on safety aspects of various recovery options it will be highly useful.
2.In case of Ethyl acetate ,I request if someone can share some good reference on its reverse solubility in water and how it varies with temperature. Because while establishing this in my lab I found very interesting aspects because of hydrolysis of ethyl acetate.
Warm regards
Deepak
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