From: Edward (chemiechem$##$gmail.com)
Date: Tue May 10 2005 - 01:52:39 EDT
I think you can quench the reduction reaction with water and then
extracted with EtOAc or others organic solvent. And then you can make
it's HCl salt
Good Lucky
On 5/10/05, everybody-request$##$orglist.net <everybody-request$##$orglist.net> wrote:
> Send Everybody mailing list submissions to
> everybody$##$orglist.net
>
> To subscribe or unsubscribe via the World Wide Web, visit
> http://two.pairlist.net/mailman/listinfo/everybody
> or, via email, send a message with subject or body 'help' to
> everybody-request$##$orglist.net
>
> You can reach the person managing the list at
> everybody-owner$##$orglist.net
>
> When replying, please edit your Subject line so it is more specific
> than "Re: Contents of Everybody digest..."
>
> Today's Topics:
>
> 1. Synthetic Pages (ste caddick)
> 2. Making Amine Hydrochloride (mailbox)
> 3. SHORT TIME DISTILLATION (mailbox)
>
> ----------------------------------------------------------------------
>
> Message: 1
> Date: Fri, 6 May 2005 19:35:51 +0100 (BST)
> From: ste caddick <stephen.caddick$##$talk21.com>
> Subject: ORGLIST: Synthetic Pages
> To: everybody$##$orglist.net
> Message-ID: <20050506183551.32648.qmail$##$web86603.mail.ukl.yahoo.com>
> Content-Type: text/plain; charset="iso-8859-1"
>
> Dear Colleagues,
>
> I wanted to make you all aware of an interactive database for synthetic chemistry. It is named synthetic pages and can be found at www.syntheticpages.org
>
> It is an interactive database in which the community can provide procedures and protocols in synthetic chemistry. It is freely available and has a nice feature of being able to have comments appended to aid the development of updated protocols - so procedures can be refined by the community. Synthetic pages has been designed to try and facilitate the transfer of information between synthetic scientists. Please feel free to use this, to join and to lodge your own pages on the site.
>
> There are currently around 200 pages on the site but plenty of opportunities for additional submission.
>
> Best wishes
>
> Stephen Caddick
>
> ---------------------------------
> How much free photo storage do you get? Store your holiday snaps for FREE with Yahoo! Photos. Get Yahoo! Photos
> -------------- next part --------------
> An HTML attachment was scrubbed...
> URL: http://two.pairlist.net/pipermail/everybody/attachments/20050506/8bc99488/attachment-0001.html
>
> ------------------------------
>
> Message: 2
> Date: Sun, 8 May 2005 10:57:46 +0530
> From: "mailbox" <mailbox$##$prolificint.com>
> Subject: ORGLIST: Making Amine Hydrochloride
> To: <everybody$##$orglist.net>
> Message-ID: <000a01c5538e$ab520db0$3be5bbcb$##$kamal>
> Content-Type: text/plain; charset="iso-8859-1"
>
> Dear Friends,
>
> I've done one reaction making Amine Hydrochloride thro' reduction of Oxime with Sodium Metal in n-Propanol. After reduction, TLC shows complete conversion of Oxime to the Amine. Now during this reaction, Sodium-n-Propoxide is also being generated as by-product.
>
> Then I passed HCl gas (also tried n-Propanol HCl) in the post reduction mixture so the Amine get converted to its HCl, but the reaction mixture becomes quite milky & being difficult to filter.
>
> Can anyone pls suggest me some good procedure that how I can do the Amine Hydrochloride with more ease after the reduction ?
>
> Thanx in advance,
>
> Kamal Morendha
>
> -------------- next part --------------
> An HTML attachment was scrubbed...
> URL: http://two.pairlist.net/pipermail/everybody/attachments/20050508/4f9661df/attachment-0001.html
>
> ------------------------------
>
> Message: 3
> Date: Sun, 8 May 2005 11:02:00 +0530
> From: "mailbox" <mailbox$##$prolificint.com>
> Subject: ORGLIST: SHORT TIME DISTILLATION
> To: <everybody$##$orglist.net>
> Message-ID: <001701c5538f$428ef120$3be5bbcb$##$kamal>
> Content-Type: text/plain; charset="iso-8859-1"
>
> Hi to all !
>
> Can I get some detailed information about "SHORT TIME DISTILLATION" ? (NOT the "Short Path Distillation").
>
> I want to distill one Aromatic Isocyanate thro' this technique, as it is being distilled under short time to lower the decomposition. What exactly the meaning of "distilling under short time" ? How I should perform it ?
>
> Awaiting your kind replies.
>
> Thanking you,
> Kamal Morendha
>
> -------------- next part --------------
> An HTML attachment was scrubbed...
> URL: http://two.pairlist.net/pipermail/everybody/attachments/20050508/47df80be/attachment-0001.html
>
> ------------------------------
>
> _______________________________________________
> ORGLIST - Organic Chemistry Mailing List
> Website / Archive / FAQ: http://www.orglist.net
> To post a message (TO EVERYBODY) send to everybody$##$orglist.net
> To unsubscribe, send to everybody-request$##$orglist.net the message: unsubscribe your_orglist_password your_address
> List coordinator: Joao Aires de Sousa (coordinator$##$orglist.net)
>
> End of Everybody Digest, Vol 8, Issue 6
> ***************************************
>
_______________________________________________
ORGLIST - Organic Chemistry Mailing List
Website / Archive / FAQ: http://www.orglist.net
To post a message (TO EVERYBODY) send to everybody$##$orglist.net
To unsubscribe, send to everybody-request$##$orglist.net the message: unsubscribe your_orglist_password your_address
List coordinator: Joao Aires de Sousa (coordinator$##$orglist.net)
This archive was generated by hypermail 2.1.4 : Tue May 10 2005 - 08:37:13 EDT