ORGLIST: ac id to acid chloride (Gholam Reza. Mashayekhi)

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From: José Barros (zerozero43$##$yahoo.com.br)
Date: Wed Apr 20 2005 - 17:01:24 EDT



Dear Mr. Mashayekhi,

there are aseveral reagents to do this. You can use
PCl3 and CCl4, Acetyl Chloride, SOCl2, (COCl)2, or
even Trichloro Isocyanuric acid (TCCA), which is very
cheap and used as chlorinating agent for pools. You
can buy it in the supermarket.

See these references:

Barstow, L. E., Hruby, V. J., J. Org. Chem. (1971)
36, 1305-1307.

Almeida, J. F., Anaya, J. Martin, N. Grande, M.,
Moran, J. R. Caballero, M. C. Tetrahedron Asymmetry
(1992) 3, 1431-1440.

Hwang, Y. C., Fowler, F. W., J. Org. Chem. (1985) 50,
2719-2726.

Hiegel, G. A., Ramirez, J., Barr, R. K., SYNTHETIC
COMMUNICATIONS 29 (8): 1415-1419 1999
 
Lynch, J. E. J. Org. Chem. (1989) 54, 3972-3782

Best regards,
José C. Barros


        
        
                
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