RE: ORGLIST: help regarding 2-4-Phenoxyphenoxy ethylamine

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From: Yuehui Zhou (yuehuizhou$##$hotmail.com)
Date: Sat Jan 22 2005 - 16:31:45 EST


The amine is not basical enough. You may try to use some stronger bases to deprotonate the amine. Sodium hydride may be the first choice. Good luck!

>From: Raman Parkesh <parkesh101@yahoo.com>
>To: everybody@orglist.net
>Subject: ORGLIST: help regarding 2-4-Phenoxyphenoxy ethylamine
>Date: Sat, 22 Jan 2005 05:14:35 -0800 (PST)
>
>
>I am trying to synthesise 2-4-Phenoxyphenoxy ethylamine by the
> > reduction of corresponding nitrile. mass spec is good but nmr is
>quite
> > messy and further the amine does not undergo boc protection. Does
> > anyone know some better method for it. Any suggestion is welcome
> > raman
>
>

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