ORGLIST: ketal synthesis

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From: José Barros (zerozero43$##$yahoo.com.br)
Date: Wed Dec 15 2004 - 20:51:09 EST


Dear all,

Did someone have problems to make a ketal of tartaric
acid using 2,2-dimethoxypropane??

I've tried the procedure of Org. Syn. (Annual Volume
68, page 92) but in fact, I obtained a kind of black
product, I don't know if the product decomposes or
polimerises.
  
Best regards
J.C. Barros.
  

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