ORGLIST:BINAP Chiral analysis

Date view Thread view Subject view Author view Attachment view

From: ROUSSEL Christian (roussel$##$spi-chim.u-3mrs.fr)
Date: Mon Sep 29 2003 - 08:36:40 EDT

Dear Peter

According to CHIRBASE database http://chirbase.u-3mrs.fr analysis of BINAP
was done as phosphine oxide by Sekar, G.; Nishiyama, H.; J. Am. Chem.
Soc., 123, 3603-3604, 2001. on Chiralpak AD column
(tris(3,5-dimethylphenyl)carbamoyl amylose coated on silica). The retention
were 10.4 and 13.6 minutes for S and R form respectively. (Eluent 75:25
Hexane / 2-PrOH) flow 0.5 mL/min Temp RT.
best Wishes

CR

Pr. Christian Roussel
ENSSPICAM, Ave Escadrille Normandie-Niemen
13397 Marseille CEDEX 2O France
tel 00 33 (0)4 91 28 82 57
Fax 00 33 (0)4 91 02 77 76
_______________________________________________
ORGLIST - Organic Chemistry Mailing List
Website / Archive / FAQ: http://www.orglist.net
To post a message (TO EVERYBODY) send to everybody$##$orglist.net
To unsubscribe, send to everybody-request$##$orglist.net the message: unsubscribe your_orglist_password your_address
List coordinator: Joao Aires de Sousa (coordinator$##$orglist.net)

Date view Thread view Subject view Author view Attachment view

This archive was generated by hypermail 2.1.4 : Wed Oct 01 2003 - 10:37:01 EDT