Re: ORGLIST:AMINE WORK-UP

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From: Yuehui Zhou (yuehuizhou$##$hotmail.com)
Date: Thu Jun 19 2003 - 21:08:26 EDT


Couldn't you complete the reaction? Then you just need to extract your product with an organic solvent. As much as I can remember the reaction is straightforward. 100% conversion is possible.

Y. Zhou

>From: "KHUMASH GHOR"
>To: everybody@orglist.net
>Subject: ORGLIST:AMINE WORK-UP
>Date: Thu, 12 Jun 2003 15:30:13 +0000
>
>Hi everybody.
>
>Thanks to the people that answer my last question; but i still
>having a problem with the chemical reduction of aromatic nitro
>compounds; i would like to know how can i separate the aromatic
>amine from the sludge of the reaction (nitro compound+ Fe and HCl),
>i have some ideas but i m not sure if is the right way to do it.
>
>In the bibliography only speak of the reaction but the isolation
>part its so poor. So if anybody have a good information about it i
>will be very thankful.
>
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