From: Uno Mäeorg (uno$##$chem.ut.ee)
Date: Wed Feb 05 2003 - 14:46:27 EST
Hi,
My be it is better to use an other strategy. First to prepare the
corresponding Shiff base and then reduce this. Usually both reactions are
going in very mild conditions and with good to excellent yield.
Dr. Uno Maeorg
At 11:45 AM 2/3/2003 +0800, Research Scholars,tpr wrote:
>Dear all
> I have prepared a long chain secondary amide(N-ethyl-octadecylamide).
>I want to reduce this to the corresponding sec. amine. LAH and
>DMSO+Methane sulphonic acid are not reducing this amide. if you can
>suggest any other procedure to reduce this Sec. aliphatic amide it will be
>very useful for me.
>thank you.
>
>with regards
>MSC.
>
>*******************************************************************************
>Research Scholar Email:tprscrs@
>Dr. T.P.Radhakrishnan's Group uohyd.ernet.in
>Theoretical & Material's Chemistry Group Tel:(040)-3010500
>School of Chemistry x-4827, 4750
>University of Hyderabad
>Hyderabad-500 046
>India
>*******************************************************************************
>
>
>
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