From: Chapman, Robert D (ChapmanRD$##$navair.navy.mil)
Date: Thu Nov 21 2002 - 16:59:00 EST
http://www.google.com/search?as_qdr=all&q=+schlenk+tube+wilhelm
provides the Internet reference
http://www.chem.yorku.ca/NAMED/PDF-FILES/Lab.pdf
which contains
"Schlenk tube, Schlenk flask
Schlenk, W.; Thal, A. Chem. Ber. 1913, 46, 2840"
Robert D. Chapman, Ph.D.
Chemistry & Materials Division
Naval Air Warfare Center
China Lake, CA 93555 USA
> ----------
> From: zabicky$##$bgumail.bgu.ac.il
> Sent: November 21, 2002 12:37 AM
> To: everybody$##$orglist.net
> Subject: ORGLIST:Schlenk
>
> Dear Orglisters,
>
> Publications dealing with very reactive organolithium compounds
> frequently
> write in their experimental section about having worked under "Schlenk
> conditions," probably meaning very low temperatures, extreme dryness of
> glassware, reagents, solvents, and the inert atmosphere for total
> exclusion
> of air (something else missing?). However, I haven't seen a direct
> citation
> of the literature source where Schlenk (I surmise W. Schlenk and E.
> Bergmann) describes the experimental setup that has been so frequently
> emulated. Can somebody point where can I find the original conditions?
>
> Thanks in advance,
>
> Jacob
>
> x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x
> Prof. Jacob Zabicky
> Institutes for Applied Research
> Ben-Gurion University of the Negev Private: POB 12366, Beer-Sheva
> 84863
> POB 653, Beer-Sheva 84105, ISRAEL Tel. +972-8-6496792
> http://profiler.bgu.ac.il/site/main.cfm
> Tel. +972-8-6461271/6461062/6472754
> Fax. +972-8-6472969
> x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x-x
>
>
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