From: Filip Stefaniak (filips$##$irc.pl)
Date: Thu May 23 2002 - 12:54:46 EDT
Hello!
I have some problems with preparing methallyl dichloride
(3-Chloro-2-chloromethyl-1-propene), H2C=C(CH2Cl)2 according to the
recepture from J. Org. Chem 2000 /by Dailey/.
I'm able to achive yield 12% instead of 50% given in the article. This
yield is independent of the scale of the reaction.
If someone has any experiences with this method please mail me - filips$##$irc.pl
Than in advance,
Regards,
filips
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