ORGLIST: Glycopeptides query

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From: patricia.Durieux (Patricia.Durieux$##$ico.unil.ch)
Date: Tue Jun 12 2001 - 12:29:02 EDT


Hi,

I'm working on sulfated glycopeptides.
I've a problem to characterize one of them.
The problem is the small quantity of my product: I can't
do TLC and I can't detect it by ElectroSprayMass Spectrometry
neither by MaldiTOF Mass Spectrometry because I think some degradations occur
(due to the Mass conditions).
I've not tried the FAB-Mass for the moment.

How can I characterize it?

Some sugars are more sensitive to conditions used
to perform a Maldi Mass Spectrum than other sugars?

Thanks.

Patricia Durieux






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