From: Mitsuhiko FUJIWHARA (pxk12345$##$nifty.ne.jp)
Date: Tue Mar 28 2000 - 05:21:54 EST
In the mail "ORGLIST: BuLi", =?ISO-8859-15?Q?Olga_T=A8ubrik?= <
olga7$##$ut.ee> wrote;
> Or can somebody advice me something better?
I think that double titlarion should be the most reliable, but I
usually don't do that practice. What I do is 1,10-phenanthroline
method. If you have access to "Lancaster" catalogue, there is the
reference for this method. I quote only one reference here: J.
Organomet. Chem. vol 9, 165 (1967). It's not so reliable, but quite
convenient and enough for usual organic synthesis. It is said that
we cannot use this method for MeLi.
____________________________________________________________________
Mitsuhiko FUJIWHARA, Ph.D. Fine & Aroma Chemical Laboratory
Takasago International Corporation
PGP-key http://www.asahi-net.or.jp/~bj9m-fjwr/index.html
PGP FingerPrint [6087 4106 3402 2D84 489B 1A83 582B 7B82 F8EB 3590]
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