ORGLIST: About GC, GC(LC)/MS analysis over Cl-NO comp.

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From: AnGio' (andrea.giordano$##$mlib.cnr.it)
Date: Fri Mar 24 2000 - 16:07:18 EST

hello all!

Does anybody of you have experience on GC, GC/MS, or LC/MS performed over
chloro-nitroso compounds? If so, what raccomandations would you give me for
such analitical procedures? I am trying to detect some gem Cl-NO compounds
obtained from short aliphatic beta-keto esters, having so far done some
GC/MS runs, but gaining little reproducibility...(by the way, those comp.
should be somehow fragile at normal condition for GC/MS, shouldn't they?)

Any kind of suggestion is welcome!

Thanks very much,
andrea.
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