ORGLIST: Quantitative NMR

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From: Jonas Nilsson (jonni$##$ifm.liu.se)
Date: Thu Feb 24 2000 - 03:20:40 EST

I need a good, none volatile, D2O-soluble NMR-additative for quantifying
in H-NMR.
I was thinking of adding a saturated D2O-solution of hexamethyldisiloxane
((Me3Si)2O). I do not think however that D2O will dissolve very much of
the reagent. I've got peaks between 1.0-2.4 ppm only.

I was thinking something like DMSO, dioxane or ethyleneglycol maybe.
/jN 

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