Re: ORGLIST: hand-made combines and distillators

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From: Christopher Paul Borella (cborella$##$ic.sunysb.edu)
Date: Tue Jan 18 2000 - 09:56:18 EST

Dear Ilfir,
The kulgaror (bulb to bulb distilation) in my opinion is the best
apparatus for distilling small quantuities under vacume, however it
normally requires specialized equipment. I have seen a couple of "home
made" versions though. The glasware is rather simple, and the heating
unit can be made from an old cannister coffee pot and the turning
mechanism can be made from many different things ranging from a old
windshield wiper mechanism to a rotovapor motor. I don't have the
specifics of how to put this together as all of ours are store bought, but
am willing to try to help whereever I can.

Regards,

Chris

On Tue, 18 Jan 2000, Ilfir R. Ramazanov wrote:

>
> Dear Orglist members,
>
> Has anyone a experience to distillate (and separate) under vacuum
> small quantities (0.5-2.0 ml) of liquid organic compounds. Yes, there
> are many special columns but I haven't ones. I am interested in
> hand-made apparatus without fine work. I'd like to hear your opinion.
>
> Best regards,
> Ilfir R. Ramazanov, Ph.D.,
> Laboratory of Catalytic Synthesis,
> Institute of Petrochemistry and Catalysis,
> pr. Oktyabrya, 141,
> Ufa, 450075, Russia.
>
> mailto:elf$##$anrb.ru
>
> Visit my homepage and find some QC software
> http://members.tripod.com/~ChemELF
>
> Visit our lab web page
> http://organomet.cjb.net
>
> 18.01.00 15:18
>
>
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>
> ORGLIST - Organic Chemistry Mailing List
> Website and Archive: http://www.orglist.net/
> List coordinator: Joao Aires de Sousa (jas$##$mail.fct.unl.pt)
>

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